286 Gooch and Blake — Estimation of Bromic Acid 



Table I — Continued. 

 Volume not exceeding 200"=™^. 







H0SO4 









AS0O3 



Error in 



KBrOg 



AS2O3 



(1:1) 



Time of 



AsoOs 



oxi- 



terms of 



taken. 



taken. 



taken 



diges- 





unchanged. 



dized. 



KBrOa. 



grm. 



grm. 



ems. 



tion. 





grm. 



grm. 



grm. 







Heated at the boiling 



temperature. 





0-1400 



0-6188 



5 



15 



min. 



0-3712 







-2476 



0-0008- 



0-1400 



0-4950 



3-5 



15 



(( 



* 0-2480 







2470 



0-0010— 



0-1400 



0-4950 



3-5 



15 



iC 



0-2482 







2468 



0-0011- 



[0-1400 



0-4950 



2-5 



15 



i( 



0-2629 







2321 



0-0097-] 



0-0700 



0-2475 



5 



15 



u 



0-1240 







1235 



0-0005 — 



0-0700 



0-2475 



5 



15 



a 



0-1239 







1236 



0-0004 — 



0-0700 



0-2475 



5 



15 



u 



0-1258 







1217 



0-0015 — 



0-0700 



0-2475 



5 



15 



u 



0-1244 







1231 



0-0007 — 



0-0700 



0-2475 



5 



10 



u 



0-1239 







1236 



0-0004- 



0-0700 



0-2475 



5 



10 



iC 



0-1237 



0- 



1238 



0-0003 — 



0-0700 



0-1584 



5 



10 



a 



0-0345 







1239 



0-0003- 



0-0700 



01584 



5 



10 



u 



0-0357 







1227 



0-0009- 



0-0700 



0-1584 



5 



10 



a 



0-0356 







1228 



0-0009- 



0-0700 



0-1584 



5 



10 



i( 



0-0353 







1231 



0-0007- 



0-0700 



0-1881 



5 



10 



(C 



0-0649 







1232 



0'0007~- 



0-0700 



0-1881 



5 



10 



i( 



0-0640 







1241 



0-0002 — 



0-0700 



0-1881 



5 



10 



u 



0-0649 







1232 



0-0007- 



0-0700 



0-1881 



5 



5 



a 



0-0652 







1229 



00008 — 



0-0700 



0-1881 



5 



5 



u 



0-0652 







1219 



0-0008 — 



0-0700 



0-2475 



2-5 



10 



a 



0-1238 







1237 



0-0004- 



0-0700 



0-2475 



2 



10 



a 



0-1235 







1240 



0-0002- 



0-0700 



0-2475 



1-15 



10 



i( 



0-1242 



0- 



1233 



0-0006- 



0-0700 



0-2475 



1-15 



10 



(( 



0-1240 







1235 



0-0005- 



[0-0700 



0-2475 



1-15 



5 



a 



0-1300 



0-1175 



00038—] 







Heated on the steam -bath -80° 







0-1400 



0-4950 



10 



150 



Qiin. 



0-2476 



0-2474 



0-0008- 



0-1400 



0-4950 



10 



150 



(( 



0-2476 



0-2474 



0-0008- 



0-1400 



0-4950 



4 



240 



a 



0-2473 



0-2477 



0-0007- 



0-1400 



0-4950 



4 



240 



a 



0-2475 



0-2475 



0-0008 — 



0-1400 



0-4950 



4 



180 



i( 



0-2472 



0-2478 



0-0006 — 



0-1400 



0-4950 



4 



180 



a 



0-2470 



0-2480 



0-0005 — 



0-1400 



0-4950 



3-5 



90 



(C 



0-2475 



0-2475 



0-0008- 



0-1400 



0-4950 



3-5 



90 



u 



0-2476 



0-2474 



0-0008— 



[0-0700 



0-2475 



1-15 



^0 



(( 



0-1622 



0-0853 



0-0217—] 







Digested at the ordinary temperat 



ure. 





0-1400 



0-4950 



4- 



46 hrs. 



0-2480 



0-2470 



0-0005- 



0-1400 



0-4950 



3-5 



41 



a 



0-2475 



0-2475 



0-0008- 



0-1400 



0-4950 



3-5 



41 



u 



0-2470 



0-2480 



0-0005 — 



0-1400 



0-4950 



3-5 



17 



i( 



0-2490 



0-2460 



0-0016— 



0-1400 



0-4950 



3-5 



17 



(I 



0-2492 







-2458 



0-0017- 



