Quantitative Determinations. 
415 
ETHTL ACETOACETATE. 
The solvent employed was from Schuchardt, and was rectified 
be distillation. The portion which boiled between 174° and 176° C. 
at 736 mm. pressure was used. The specific conductivity was 
4 X 10- 7 . 
Table XVI. 
Solvent: 
ethyl acetoacetate. 
Ferric Chloride, 
Antimony Trichloride, 
Fe Cl 
3* 
Sb Cl 3 . 
V 
M 
V 
M 
5.46 
10.82 
0.75 
0.031 
15.04 
14.04 
0.94 
0.034 
16.31 
14.08 
1.34 
0.041 
22.14 
14.62 
2.76 
0.044 
24.12 
14.63 
4.34 
0.050 
27.59 
15.04 
8.18 
0.059 
31.90 
15.25 
17.02 
0.076 
44.64 
15.94 
33.69 
0.108 
157.98 
19.79 
59.86 
0.132 
240.51 
20.65 
511.50 
0.529 
503.56 
23.43 
Mercuric Chloride, 
Ferric Chloride, 
Hg Cl 
8* 
(v =5.46 at 25° C. 
Solution two weeks old.) 
V 
M 
t 
n 
0.91 
0.012 
25° C 
12.0 
1.35 
0.013 
50 
16.8 
2.91 
0.017 
56 
17.5 
36.33 
0.072 
60 
18.2 
65 
19.2 
Phosphorus Trichloride, 
70 
19.9 
PC1 3 
75 
20.7 
V 
M 
81 
21.2 
1.80 
0.026 
86 
21.7 
4.48 
0.097 
90 
21.7 
95 
21.8 
Stannic Chloride, 
100 
21.7 
SnCl 
4* 
(Gases disengaged 
V 
M 
at higher temperatures.) 
2.02 1.08 
4.13 1.71 
8.76 2.37 
